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Process Variations in Microsystems Manufacturing
Michael Huff
Verlag Springer-Verlag, 2020
ISBN 9783030405601 , 531 Seiten
Format PDF, OL
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Preface
7
Acknowledgments
10
Contents
11
Chapter 1: Introduction
18
1.1 From Vacuum Tubes to Microsystems
18
1.2 MEMS Microsystems
19
1.3 Some of the Important Attributes of MEMS Microsystems
21
1.4 Organization of This Book
23
References
25
Other Information
25
Chapter 2: An Overview of MEMS Microsystems
26
2.1 Introduction
26
2.2 Microsensors and Microactuators
26
2.2.1 MEMS Microsensors
27
2.2.1.1 Resistive
27
2.2.1.2 Piezoresistive
29
2.2.1.3 Capacitive
30
2.2.1.4 Piezoelectric
32
2.2.1.5 Tunneling
33
2.2.1.6 Magnetic
35
2.2.1.7 Photoconduction
36
2.2.1.8 Thermoelectric
37
2.2.1.9 Diodes
38
2.2.2 MEMS Microactuators
40
2.2.2.1 Electrostatic
40
2.2.2.2 Piezoelectric
41
2.2.2.3 Thermal
43
2.2.2.4 Shape-Memory Alloys (SMA)
44
2.2.2.5 Magnetic
45
2.3 Microsystems Manufacturing Processes
47
2.4 Batch Fabrication
49
2.5 Some Basics of Microsystems Manufacturing
51
2.5.1 Differences Between IC and MEMS Manufacturing
52
2.5.2 Microsystems Feature Sizes
54
2.6 Some Material Basics Regarding Semiconductors and Silicon
55
2.7 Summary
60
References
60
Chapter 3: Microsystems Manufacturing Methods: Integrated Circuit Processing Steps
62
3.1 Introduction
62
3.2 Basic IC Processing Steps
64
3.2.1 Thin-Film Growth and Deposition Techniques
64
3.2.1.1 Thermal Oxidation
64
3.2.1.2 Chemical Vapor Deposition
69
3.2.1.2.1 Atmospheric Chemical Vapor Deposition (ACVD)
72
3.2.1.2.2 Low-Pressure Chemical Vapor Deposition (LPCVD)
73
3.2.1.2.3 Plasma-Enhanced Chemical Vapor Deposition (PECVD)
75
3.2.1.2.4 Atomic Layer Deposition (ALD)
77
3.2.1.3 Physical Vapor Deposition (PVD)
79
3.2.1.3.1 Evaporation
79
3.2.1.3.2 Sputtering
82
3.2.2 Impurity Doping
84
3.2.2.1 Thermal Diffusion
85
3.2.2.2 Ion Implantation
88
3.2.3 Photolithography
93
3.2.4 Rapid Thermal Anneal (RTA)
98
3.2.5 Planarization
100
3.2.6 Etching
102
3.2.7 Clean and Strip
109
3.3 Summary
110
References
111
Chapter 4: Microsystems Manufacturing Methods: MEMS Processes
115
4.1 Introduction
115
4.2 MEMS Substrate Material Types
116
4.3 MEMS Materials Deposition Processing Steps
117
4.3.1 MEMS Thin-Film Materials Deposited on IC Equipment
117
4.3.1.1 Thin-Film Semiconductors
117
4.3.1.1.1 Silicon (Si)
117
4.3.1.1.2 Silicon-Germanium (SiGe)
119
4.3.1.1.3 Germanium (Ge)
120
4.3.1.1.4 Silicon Carbide (SiC)
120
4.3.1.1.5 Diamond
121
4.3.1.2 Metals
122
4.3.1.3 Thin-Film Metal Oxides
124
4.3.1.4 Dielectrics
125
4.3.1.4.1 Silicon Nitride (SiN)
125
4.3.1.4.2 Silicon Dioxide (SiO2)
126
4.3.1.5 Polymers
127
4.3.1.5.1 SU-8
127
4.3.1.5.2 PDMS
128
4.3.1.5.3 Polyimide
128
4.3.1.6 Ceramics
129
4.3.1.7 Special MEMS Materials
130
4.3.1.7.1 Piezoelectric Materials
130
4.3.1.7.2 Shape-Memory Alloys (SMAs)
132
4.3.1.7.3 Magnetic Materials
133
4.3.2 MEMS Specific Processing Steps
134
4.3.2.1 Electrochemical Deposition
134
4.3.2.2 MEMS Lithography
136
4.3.2.2.1 Contact Photolithography
137
4.3.2.2.2 Front-to-Back Contact Photolithography
137
4.3.2.2.3 Direct-Write Laser Photolithography
138
4.3.2.2.4 Grayscale Photolithography
138
4.3.2.2.5 X-Ray Lithography
140
4.3.2.2.6 E-Beam Lithography
140
4.3.2.2.7 Lithography on Large Topography
141
4.3.2.2.8 Lift-Off Patterning
142
4.3.2.2.9 Image Reversal Photoresists
143
4.3.2.2.10 Photolithography on Transparent Substrates
144
4.4 MEMS Micromachining Methods
144
4.4.1 Bulk Micromachining
145
4.4.1.1 Wet Chemical Etchants
145
4.4.1.1.1 Isotropic Wet Chemical Etchants
146
4.4.1.1.2 Anisotropic Wet Chemical Etchants
147
4.4.1.2 Gas-Phase Isotropic Chemical Etchants
153
4.4.1.3 Deep Reactive Ion Etching (DRIE) of Silicon
154
4.4.1.4 Deep, High-Aspect Ratio RIE of Fused Silica, Quartz, and Glass
157
4.4.1.5 Deep, High-Aspect Ratio RIE of Silicon Carbide (SiC)
159
4.4.2 Surface Micromachining
160
4.4.3 Wafer Bonding
163
4.4.4 LIGA
166
4.4.5 Hot Embossing
168
4.4.6 Other MEMS Micromachining Technologies
169
4.4.6.1 Electro-Discharge Micromachining
169
4.4.6.2 Laser Micromachining
169
4.4.6.3 Focused Ion Beam (FIB) Micromachining
170
4.4.6.4 Electrochemical Fabrication (EFAB)
171
4.5 Summary
171
References
173
Chapter 5: Metrology for Microsystems Manufacturing
188
5.1 Introduction
188
5.2 Fabrication Metrology Equipment and Methods
189
5.2.1 Optical Microscopy
189
5.2.2 Fluorescence Microscopy
192
5.2.3 Confocal Microscopy
194
5.2.4 Stereomicroscopy
195
5.2.5 Scanning Electron Microscope (SEM)
195
5.2.6 Automated Scanning Electron Microscope
198
5.2.7 Thin-Film Thickness
200
5.2.7.1 Interferometry
200
5.2.7.2 Ellipsometry
202
5.2.7.3 Stylus Profilometry
204
5.2.8 Four-Point Probe
206
5.2.9 Thin-Film Stress Measurement
208
5.2.10 Particle Measurements
212
5.2.11 Noncontact Optical Profilometry
213
5.2.12 Wafer Bonding Inspection
215
5.3 Specialized Metrology Equipment and Methods
218
5.3.1 Focused Ion Beam
218
5.3.2 Scanning Tunneling Microscopy (STM)
221
5.3.3 Atomic Force Microscopy (AFM)
223
5.3.4 Energy-Dispersive X-Ray Spectroscopy (EDXS)
225
5.4 Highly Specialized Material Analysis Methods
227
5.5 Electrical Material Properties Test Methods
232
5.5.1 Junction Depth Measurements
232
5.5.2 Spreading Sheet Resistance
233
5.6 Summary
236
References
238
Chapter 6: Microsystems Material Properties
241
6.1 Introduction
241
6.2 Residual Stress and Young´s Modulus
243
6.2.1 Young´s Modulus
244
6.2.2 Residual Stress
246
6.3 Mechanical Test Structures
248
6.3.1 Test Structures for Young´s Modulus
248
6.3.2 Thin-Film Residual Stress Test Structures
251
6.3.3 Stress Gradients
255
6.3.4 Tests for Other Mechanical Material Properties
256
6.4 Electrical Test Structures
257
6.5 Thin-Film Material Properties
264
6.5.1 Thermal SiO2
264
6.5.2 LPCVD Polysilicon
265
6.5.3 LPCVD Silicon Dioxide (SiO2)
269
6.5.4 LPCVD Silicon Nitride (SiN)
271
6.5.5 PECVD Silicon Dioxide (SiO2)
273
6.5.6 PECVD Silicon Nitride (SiN)
275
6.5.7 PECVD Polycrystalline Silicon
277
6.5.8 Evaporative Physical Vapor Deposition
277
6.5.9 Sputter Physical Vapor Deposition
280
6.5.9.1 Sputter-Deposited Silicon
280
6.5.10 Electrochemical Deposition
281
6.6 Summary
283
References
283
Chapter 7: Microsystems Process Integration, Testing, and Packaging
288
7.1 Introduction
288
7.2 What Is Process Integration?
289
7.3 How Is Process Integration Performed?
291
7.4 What Is an Integrated MEMS Process Sequence?
296
7.5 Examples of MEMS Microsystems Process Technologies
296
7.5.1 PolyMUMPS Process Technology
297
7.5.1.1 Some Important Elements About PolyMUMPS
302
7.5.2 Digital Light Processor (DLP) Technology
304
7.5.2.1 Some Key Elements About the DLP Process Technology
307
7.6 Process Integration and Manufacturing Variations
308
7.6.1 Causes of Device Parameter Variations in Process Sequences
308
7.6.2 An Example of Parameter Variations for a Process Technology: The PolyMUMPS Process
311
7.7 Microsystems Design Rules
314
7.7.1 MEMS Microsystems Design Rules
314
7.7.2 Design Rule Checking
316
7.8 MEMS Microsystems Testing
317
7.8.1 Example of MEMS Microsystems Testing
318
7.8.2 MEMS Microsystems Device Trimming
319
7.8.3 MEMS Microsystems Calibration
320
7.9 MEMS Microsystems Packaging
320
7.10 Summary
323
References
323
Chapter 8: Device Parameter Variations in Microsystems Manufacturing
325
8.1 Introduction
325
8.2 Manufacturing Variations
326
8.3 Measurement of Manufacturing Variations
327
8.4 Bias and Random Variations
328
8.5 Resolution, Precision, and Accuracy
331
8.6 Comparison of the Dimensional Parameter Variations in Manufacturing Technologies
333
8.7 The Nature of Random Parameter Variations
337
8.8 Discrete Probability Distributions
354
8.9 Some Examples of Statistical Analysis of Variations
357
8.9.1 Confidence Interval for Manufacturing Large Samples (N > 30)
357
8.9.2 Confidence Interval for Small Samples (N < 30)
359
8.9.3 Hypothesis Testing for Small Sample Sizes (N < 30)
359
8.9.4 Hypothesis Testing of Goodness of Fit
363
8.9.5 Sample Size Required to Estimate Population Mean
365
8.9.6 Example of Use of the Hypergeometric Distribution
366
8.9.7 Example of Poisson Distribution
366
8.10 Impact of Physics and Random Parameter Variations
367
8.11 Combination of Both Bias and Random Manufacturing Parameter Variations
371
8.12 Device Output Behavior Variation Due to Parameter Variations
373
8.13 Example of Device Output Behavior Variation Analysis
375
8.14 Simplified Variation Analysis
382
8.15 Important Generalizations
384
8.16 Review of Methods for Variation Analysis
387
8.16.1 Worst-Case Variation Analysis
389
8.16.2 Non-worst-Case Variation Analysis
393
8.16.2.1 Non-sampling, Non-worst-Case Variation Analysis
393
8.16.2.2 Monte Carlo Variation Analysis
394
8.17 Summary
398
References
399
Chapter 9: Yield Analysis and Quality Assurance and Control Methods Used in Microsystems Manufacturing
400
9.1 Introduction
400
9.2 Importance of Manufacturing Yield
401
9.3 Definitions of Microsystems Manufacturing Yield
402
9.4 Microsystems Manufacturing Yield Monitoring and Analysis
404
9.4.1 Functional Yield
405
9.4.1.1 Functional Yield Models Based on Point Defects
406
9.4.1.2 Functional Yield Measurement Tools
410
9.4.2 Parametric Yield
411
9.4.2.1 Parametric Yield Model
411
9.4.2.2 An Example of a Parametric Yield Model
419
9.5 Yield Estimations Using Sampling Methods
421
9.5.1 Yield Estimation Using Regionalization
422
9.5.2 Yield Estimation Using Simplicial Approximation
425
9.5.3 Monte Carlo Yield Estimation
428
9.5.3.1 Confidence Intervals for Monte Carlo Yield Analysis
429
9.6 Statistical Process Control (SPC)
431
9.6.1 Control Charts for Variables
435
9.6.2 Control Charts for Attributes
440
9.6.3 Identification of Non-random Patterns in Control Charts
445
9.6.4 Process Capability
446
9.6.5 Rational Subgroups
450
9.6.5.1 Sampling Methods for Rational Subgroups
454
9.7 Summary
456
References
456
Chapter 10: Managing Parameter Variations in Microsystems Device Design
458
10.1 Introduction
458
10.2 Relationships Between Process Sequence and Parameter Variations
460
10.3 Overview of MEMS Device Design and Modeling
462
10.4 Example of the Design Levels for a MEMS Device
465
10.5 MEMS Design for Manufacturability
469
10.5.1 MEMS Device Design for Manufacturability
470
10.5.2 MEMS Process Sequence Design for Manufacturability
471
10.5.3 MEMS Microsystems Partitioning
473
10.6 Overview of MEMS Development
474
10.7 MEMS Design for Manufacturability Recommendations
477
10.8 Managing Device Parameter Variations in MEMS Design
478
10.8.1 Design Centering
480
10.8.2 Parameter Variation Reduction
484
10.8.3 Device Size Scaling
486
10.8.4 Acceptance Range Increase
488
10.8.5 Best Practices in Layout Design
489
10.8.6 Further Comments About MEMS Design Methods
496
10.9 MEMS Design in Multidimensional Spaces
497
10.10 MEMS Design Methods Using Monte Carlo Techniques
502
10.10.1 Design Centering Using Monte Carlo
505
10.11 Sensitivity Analysis
509
10.11.1 Generalized Sensitivity Analysis Methods
512
10.11.2 Optimizing Manufacturing Cost Function
516
10.12 Summary
517
References
517
Index
519